• CN:11-2187/TH
  • ISSN:0577-6686

›› 2014, Vol. 50 ›› Issue (12): 171-176.

• 论文 • 上一篇    下一篇

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化学镀镍方法制备金属微孔滤膜

卢继霞;丁慧;方亮;贾瑞清   

  1. 中国矿业大学(北京)机电学院
  • 发布日期:2014-06-20

Method to Make Metal Micro-pore Filter Membrane through Electro-less Nickel-plating

LU Jixia;DING Hui;FANG Liang;JIA Ruiqing   

  1. School of Mechanical, Electronic and Information Engineering,China University of Mining and Technology
  • Published:2014-06-20

摘要: 滤膜堵塞型传感器可以半定量地评价油液的固体颗粒污染度,其关键元件为金属微孔滤膜。为了获得性价比较高的金属微孔滤膜,选择600目平纹不锈钢丝网为镀覆基材,研究所选不锈钢丝网表面化学镀镍的工艺流程,通过扫描电镜(LEO 1450 VP)和能谱分析仪(INCA ENERGY 300)分析镀层成分、镀层与基材的结合情况以及微孔滤膜的微孔及丝径尺寸。结果表明,本研究工艺下制备的微孔滤膜镀层为低磷镀层,抗拉强度为400~700 MPa,硬度为580 HV,镀层与基体材料结合牢固。镀覆20 min和30 min后可获得微孔尺寸分别为14 m和10 m的微孔滤膜,且丝径镀覆厚度均匀一致,微孔大小也均匀一致。利用所研制的金属微孔滤膜制成滤膜堵塞型传感器,配制样液分别对该传感器的重复性精度和污染度检测精度进行检验,结果表明,微孔滤膜传感器具有较好的重复性精度,对油液中固体颗粒污染度等级的测定结果与实际值完全一致,因此所研制的金属微孔滤膜可以满足滤膜堵塞型传感器的使用要求。

关键词: 滤膜堵塞型传感器;金属微孔滤膜;化学镀镍;污染度检测

Abstract: Medium-blocking-type sensor can semi-quantitatively evaluate the solid particle contamination level in oil, and the key element of this sensor is the metal micro-pore filter membrane. A new method was proposed to make the metal micro-pore filter membrane in high price/performance ratio by using electro-less nickel-plating on a kind of 600-mesh twill weave stainless steel wire meshes. The technological process of electro-less nickel-plating is well studied and summarized. Furthermore, the composition of the coating, the combination of the coating and the base material and the sizes of micro-pores and wire diameters of the micro-pore filter membrane are analyzed by scanning electron microscope (LEO 1450 VP) and spectrum analyzer (INCA ENERGY 300). The results show that the layer of the micro-pore filter membrane got by studied technological process is low-phosphorus coating with tensile strength of 400-700 MPa and hardness of 580 HV, showing the coating and the base material are combined firmly. The micro-pore filter membrane with sizes of 14 m and 10 m can be got after 20 minutes’ and 30 minutes’ nickel-plating, respectively. The thickness of the wire diameter increased uniformly, and the micro pores are almost in the same size. In order to check the quality of the micro-pore filter membrane, the repeatability accuracy and the precision in contamination level testing of a medium-blocking-type sensor made with the studied metal micro-pore filter membrane are carried out, and the results show that the medium-blocking-type sensor has good repeatability and its contamination level testing results consistent with the actual value. Therefore, the micro-pore filter membrane made through this method can meet the requirements of medium-blocking-type sensor.

Key words: medium-blocking-type sensor;metal micro-pore filter membrane;electro-less nickel-plating;contamination level testing

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