• CN:11-2187/TH
  • ISSN:0577-6686

›› 2007, Vol. 43 ›› Issue (6): 137-141.

• 论文 • 上一篇    下一篇

扫码分享

计算机硬磁盘基片表面纳米粒子冲蚀磨损

徐进;雒建斌   

  1. 清华大学摩擦学国家重点试验室
  • 发布日期:2007-06-15

VARIATIONS OF HARD DISK SUBSTRATE INDUCED BY NANOPARTICLE IMPACTS

XU Jin;LUO Jianbin   

  1. State Key Laboratory of Tribology, Tsinghua University
  • Published:2007-06-15

摘要: 为探讨磁盘片表面NiP涂层在颗粒冲击过程中的碰撞损伤及与冲蚀时间的关系,利用高分辨透射电镜、原子力显微镜、X射线光电子能谱仪和俄歇电子能谱仪等考察计算机硬磁盘基片表面NiP涂层经含SiO2纳米颗粒抛光液冲击后发生的微观物理变化。结果表明:经纳米颗粒碰撞后的计算机硬磁盘基片表面NiP涂层损伤随碰撞时间明显变化,在经颗粒碰撞后的表面上可观测到颗粒嵌入、纳米尺度的凹坑和划痕;NiP涂层表面在碰撞过程中发生氧化,氧化程度随时间延长而加剧。经3 min抛光液冲击后,在表面以下大约6 nm深度可观测到P元素的聚集,在涂层的亚表面可观测到纳米尺度的晶粒,晶粒的尺寸受冲击时间的影响。

关键词: NiP涂层, 计算机硬磁盘片, 纳米颗粒碰撞, 抛光

Abstract: In order to investigate the damage of the nickel- phosphorous (NiP) coating the surface on computer hard disk substrate after SiO2 nanoparticle impact, a test of nanoparticle impact on a hard disk substrate with the NiP coating is carried out and the variation of the microstructure of the impacted surface is examined by using a high resolution transmission electron microscope (HRTEM), an atomic force microscope (AFM), an auger electron spectrogram (AES), and an X-ray photoelectron spectroscopy (XPS). The experimental results indicate that lots of fine craters and scratches in the nano-scale can be seen on the impacted surface, and some nanoparticles can be embedded in the surface during the impacts. HRTEM observations from the cross-section specimen under different test conditions show the existence of nano-crystalline transformation in the subsurface layer after the impact, and the sizes of these crystalline relate closely to the exposure time. Nanoparticle impacts aggravate the oxidation of the Ni-P alloy coating, and the impact with an exposure time of three minutes promotes the concentration of element phosphorus in the subsurface below about 6 nm.

Key words: Computer hard disk, Nanoparticle impact, NiP coating, Polishing

中图分类号: