• CN:11-2187/TH
  • ISSN:0577-6686

›› 2013, Vol. 49 ›› Issue (11): 121-127.

• 论文 • 上一篇    下一篇

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低能电子束原位固化树脂基复合材料纤维铺放制造及性能研究

赵新明;段玉岗;刘潇龙;张小辉;李涤尘   

  1. 西安交通大学机械制造系统国家重点实验室;装甲兵技术学院机械工程系
  • 发布日期:2013-06-05

Fabrication and Properties of Polymer Matrix Composites by Low-energy Electron Beam In-situ Cured Fiber Placement Process

ZHAO Xinming;DUAN Yugang;LIU Xiaolong;ZHANG Xiaohui;LI Dichen   

  1. State Key Lab for Manufacturing Systems Engineering, Xi’an Jiaotong University Department of Mechanical Engineering, Armored Institute of Technology
  • Published:2013-06-05

摘要: 针对树脂基复合材料热压罐固化能耗高、工艺周期长以及高能电子束固化辐射大,设备笨重等问题,研究125 keV低能电子束与纤维铺放相结合的复合材料原位固化分层制造方法及复合材料性能。试验结果表明,125 keV低能电子束穿透能力较差,在辐照固化过程中电子能量衰减很大,不能穿透0.125 mm单层预浸带,双面辐照能够穿透复合材料预浸带且辐照剂量分布均匀。由于低能电子束固化过程温度低,即使辐照剂量达到250 kGy,固化度及玻璃化转变温度仍然只有60.7%和48.3 ℃。但经加热后固化处理后,复合材料的固化度及玻璃化转变温度得到了大幅度提高,50 kGy双面辐照复合材料层压板经180 ℃加热30 min后固化处理,其固化度从16.7%上升到97.4%, 玻璃化转变温度从–3.2 ℃提高到167.3 ℃,同时试验结果表明经50 kGy双面辐照及热后固化复合材料的层间抗剪强度达到59.62 MPa,接近高能电子束固化复合材料层间抗剪强度。

关键词: 层间抗剪强度, 低能电子束, 分层制造, 复合材料, 纤维铺放

Abstract: The stepwise fabrication method combines 125 keV low energy electron beam and fiber placement for polymer matrix composites is investigated to reduce the high energy consumption and curing time of the auto-clave process and to overcome the high shield investment of the high energy electron beam process, the properties of the composites is also evaluated. The experimental results show that the 125 keV electron beam can not penetrate the single layer prepreg with the thickness of 0.125 mm due to its low energy. But the consistent irradiation can be gotten in the prepreg by both-side irradiation. Because of the very low temperature of the prepreg during the irradiation process, the degree of curing and the glass transition temperature of the composites at the 250 kGy irradiation does level are only 60.71% and 48.34 ℃, respectively. But after heat postcure, the degree of curing and the glass transition temperature of the composites increase significantly. After being treated at 180 ℃ for 30 min, the degree of curing of the composites laminate irradiates both-side with 50 kGy does increased from 16.7% to 97.4%, and the glass transition temperature increases from –3.2 ℃ to 167.3 ℃, respectively. The test results exhibit that the interlaminar shear strength of the laminate is cured by low energy electron beam and heat treatment reaches 59.62 MPa, which is close to that of the composite laminate cured by high energy electron beam.

Key words: Composites, Fiber placement, Interlaminar shear strength, Low-energy electron beam, Stepwise fabrication

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