38CrMoAl液压柱塞无白亮层低温离子渗氮工艺研究

doi:10.3901/JME.2017.22.081

机械工程学报 ›› 2017, Vol. 53 ›› Issue (22): 81-86.doi: 10.3901/JME.2017.22.081

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38CrMoAl液压柱塞无白亮层低温离子渗氮工艺研究

陈尧¹, 宋磊¹, 张宸恺¹, 叶雪梅², 胡静¹

1. 常州大学江苏省材料表面科学与技术重点实验室常州 213164;
2. 江苏恒立高压油缸股份有限公司常州 213134

收稿日期:2016-09-02 修回日期:2017-05-24 出版日期:2017-11-20 发布日期:2017-11-20
通讯作者: 胡静(通信作者),女,1966年出生,博士,教授,硕士研究生导师。主要研究方向为金属材料表面改性。E-mail:jinghoo@126.com
作者简介:陈尧,女,1993年出生。主要研究方向为金属表面改性。E-mail:CZ125115@163.com
基金资助:
江苏省科技成果转化（BA2013078）和江苏省研究生创新基金资助项目。

Lower Temperature Plasma Nitriding without White Layer for 38CrMoAl Hydraulic Plunger

CHEN Yao¹, SONG Lei¹, ZHANG Chenkai¹, YE Xuemei², HU Jing¹

1. Jiangsu Key Laboratory of Materials Surface Science and Technology, Changzhou University, Changzhou 213164;
2. Jiangsu Hengli High Pressure Oil Cylinder Co., Ltd., Changzhou 213134

Received:2016-09-02 Revised:2017-05-24 Online:2017-11-20 Published:2017-11-20

摘要/Abstract

摘要： 对38CrMoAl液压柱塞进行低温离子渗氮，研究不形成白亮层的工艺条件。采用金相显微镜、X射线衍射仪、显微硬度计、摩擦磨损试验机对处理后的38CrMoAl钢显微组织、截面硬度、渗层脆性、耐磨性进行了分析。研究结果表明，相比于510℃常规离子渗氮工艺，38CrMoAl钢经450℃低温离子渗氮工艺处理后无白亮层产生，X射线衍射分析表明表层无γ'-Fe₄N相生成。同时，38CrMoAl钢经450℃低温离子渗氮工艺处理后，不仅截面硬度满足使用要求，而且渗层脆性显著降低，压痕周围均无裂纹产生。耐磨性研究表明，在较大载荷下，450℃低温离子渗氮后耐磨性比510℃常规离子渗氮好。

关键词: 38CrMoAl, 白亮层, 离子渗氮, 液压柱塞

Abstract: Lower temperature plasma nitriding is conducted for 38CrMoAl hydraulic plunger in this research. Optical microscopy (OM),X-ray diffraction(XRD) and micro-hardness and wear tester are used to investigate the microstructure,surface hardness,brittleness of modified layer and wear resistance. The results show that no white bright layer is formed while plasma nitriding at 450℃ for 6 h,and XRD also confirm that there existed no γ'-Fe₄N phase. Meanwhile,the brittleness is decreased at lower temperature plasma nitriding comparing with conventional plasma nitriding,there existed no crack around the indentation for samples plasma nitriding at 450℃. Meanwhile,the wear resistance of samples plasma nitrided at 450℃ is higher than that of the conventional plasma nitrided samples and meet the requirements.

Key words: 38CrMoAl, hydraulic plunger, plasma nitriding, white layer

中图分类号:

TG156

陈尧, 宋磊, 张宸恺, 叶雪梅, 胡静. 38CrMoAl液压柱塞无白亮层低温离子渗氮工艺研究[J]. 机械工程学报, 2017, 53(22): 81-86.

CHEN Yao, SONG Lei, ZHANG Chenkai, YE Xuemei, HU Jing. Lower Temperature Plasma Nitriding without White Layer for 38CrMoAl Hydraulic Plunger[J]. Journal of Mechanical Engineering, 2017, 53(22): 81-86.

参考文献

[1] ALPHONSA J,RAJA V S,MUKHERJEE S. Development of highly hard and corrosion resistant A286 stainless steel THROUGH plasma nitrocarburizing process[J]. Surface & Coatings Technology,2015,280:268-276.
[2] 王春光,邓德伟,刘丹,等. 离心式压缩机齿轮的快速深层等离子渗氮[J]. 机械工程学报,2010,46(8):56-61. WANG Chunguang,DENG Dewei,LIU Dan,et al. Fast and deep case plasma nitriding of gear of centrifugal compressor[J]. Journal of Mechanical Engineering,2010,46(8):56-61.
[3] WU J,YE X,LI H,et al. A study of the influence of plasma post-oxidizing on the corrosion resistance[J]. Vacuum, 2015,111(111):110-113.
[4] PINEDO C E. The use of selective plasma nitriding on piston rings for performance improvement[J]. Materials and Design,2003,24(2):131-135.
[5] 刘小林,郑辉,杨闽红. 38CrMoAl钢大模数齿轮深层离子渗氮工艺探讨[J]. 热处理,2011,26(6):43-45. LIU Xiaolin,ZHENG Hui,YANG Minhong. Deep ion nitriding of large module gear of 38CrMoAl steel[J]. Heat Treatment,2011,26(6):43-45.
[6] 周上祺,候琼,任勤. 38CrMoAl钢离子渗氮微观结构的研究[J]. 金属热处理,2002,27(10):10-12. ZHOU Shangqi,HOU Qiong,REN Qin. Microstructure of ion nitriding layer in 38CrMoAl steel[J]. Heat Treatment of Metals,2002,27(10):10-12.
[7] 王松,岳文,王成彪,等. 渗氮GCr15钢在含氮硼酸酯添加剂润滑油作用下的摩擦学性能[J]. 机械工程学报,2012,48(9):128-133. WANG Song,YUE Wen,WANG Chengbiao,et al. Tribological properties of plasma nitriding GCr15 steel under lubrication with borate containing nitrogen additive[J]. Journal of Mechanical Engineering,2012,48(9):128-133.
[8] EBRAHIMI M,MAHBOUBI F,NAIMI-JAMAL M R. Wear behavior of DLC film on plasma nitrocarburized AISI 4140 steel by pulsed DC PACVD:Effect of nitrocarburizing temperature[J]. Diamond & Related Materials,2014,52:32-37.
[9] CHATTERJEE-FISHER R,LIETKE D,HOFFMANN R,等. 渗氮和氮碳共渗[M]. 北京:机械工业出版社,1989. CHATTERJEE-FISHER R,LIETKE D,HOFFMANN R, et al. Nitriding and nitrocarburizing[M]. Beijing:China Machine Press,1989.
[10] 刘沅东,王成彪,车延岗,等. 离子轰击热处理技术对轴承钢摩擦学性能的影响[J]. 机械工程学报,2011,47(5):126-133. LIU Yuandong,WANG Chengbiao,CHE Yangang,et al. Ttibological properties of 52100 steel treated by different plasma bombardment heat treatment method[M]. Journal of Mechanical Engineering,2011,47(5):126-133.
[11] ZHAO C,LI C X,DONG H,et al. Study on the active screen plasma nitriding and its nitriding mechanism[J]. Surface and Coatings Technology,2006,201(6):2320-2325.
[12] ZAGONEL L F,BETTINI J,BASSO R L O,et al. Nanosized precipitates in H13 tool steel low temperature plasma nitriding[J]. Surface & Coatings Technology,2012,207(21):72-78.
[13] BENDO T,MALISKA A M,ACUÑA J J S,et al. Nitriding of surface Mo-enriched sintered iron:Structure and morphology of compound layer[J]. Surface & Coatings Technology,2014,258:368-373.
[14] CHIU L H,SU Y Y,CHANG F S C H. Microstructure and properties of active screen plasma nitrided duplex stainless steel[J]. Materials & Manufacturing Processes,2010,25(5):316-323.
[15] BENDO T,MALISKA A M,ACUÑA J J S,et al. Nitriding of surface Mo-enriched sintered iron:Structure and morphology of compound layer[J]. Surface & Coatings Technology,2014,258:368-373.
[16] NAYEBPASHAEE N,SOLTANIEH M,KHEIRANDISH S. A study on formation and growth mechanism of nitride layers during plasma nitriding process of plastic injection mold steel[J]. Materials and Manufacturing Processes,2015,31(9):1192-1200.
[17] 戴达煌,周克松,袁镇海. 现代材料表面技术科学[M].北京:冶金工业出版社,2004. DAI Dahuang,ZHOU Kesong,YUAN Zhenhai. The modern surface technology science[M]. Beijing:Metallurgical Industry Press,2004.
[18] TONG W P,HAN Z,WANG L M,et al. Low-temperature nitriding of 38CrMoAl steel with a nanostructured surface layer induced by surface mechanical attrition treatment[J]. Surface & Coatings Technology,2008,202(20):4957-4963.
[19] 杨月华,冯德学. 离子氮化白亮层和渗层不合格的分析与解决[J]. 热处理技术与装备,2014,35(2):43-46. YANG Yuehua,FENG Dexue. Analysis and solution of unqualification problem about nitride layer and nitriding depth[J]. Heat Treatment Technology and Equipment,2014,35(2):43-46.

38CrMoAl液压柱塞无白亮层低温离子渗氮工艺研究

Lower Temperature Plasma Nitriding without White Layer for 38CrMoAl Hydraulic Plunger

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[1]	王松;岳文;王成彪;高晓成;卜宏利;刘家浚. 渗氮GCr15钢在含氮硼酸酯添加剂润滑油作用下的摩擦学性能[J]. , 2012, 48(19): 128-133.
[2]	刘沅东;王成彪;车延岗;袁静静;刘家浚. 离子轰击热处理技术对轴承钢摩擦学性能的影响[J]. , 2011, 47(5): 126-133.
[3]	王春光;邓德伟;刘丹;王永;关锰. 离心式压缩机齿轮的快速深层等离子渗氮[J]. , 2010, 46(8): 56-61.
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